School of Physics - Theses
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ItemDetecting and characterising extrasolar planets in reflected light(University of Melbourne, 2009)
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ItemFault-tolerant quantum computation with local interactions(University of Melbourne, 2009)
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ItemMonte Carlo characterisation of narrow photon fields for intensity modulated radiotherapy(University of Melbourne, 2006)
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ItemFocusing of an atomic beam using a TEM01 mode lens(University of Melbourne, 2006)
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ItemThe Panoramic Deep Fields( 2001)The Panoramic Deep Fields are a deep multicolour survey of two ~ 25 ° fields at high galactic latitude. The survey images have been constructed by digitally stacking scans UK Schmidt plates. Deep images (Bj ~23.5) with low contamination have been obtained by subtracting the background from the individual plates scans and using bad pixel rejection during the stacking. The size and depth of the fields allow the accurate statistical measurement of the environments and evolution of galaxies and AGN. The clustering of galaxies and galaxy clusters has been measured from z ~0.4 until the current epoch. The clustering properties of galaxies are strongly correlated with colour and blue U – Bj selected galaxies exhibit weaker clustering than any morphologically selected sample. The weak clustering (ro ≤ 3h -1 Mpc) of blue galaxies implies galaxy colour and stellar population are more strongly correlated with environment than galaxy morphology. Despite the large fields-of-view, the clustering of red galaxies and clusters varies significantly between the two fields and the distribution of clusters is consistent with this being due to large-scale-structure at z ~0.4. The evolution and environments of AGN have been measured at intermediate redshifts with the Panoramic Deep Fields. Photometric redshifts, colour selection and the NVSS have been used to compile a catalogue of ~ 180 0.10 < z< 0.55 radio galaxies. The evolution of the radio galaxy luminosity function is consistent with luminosity evolution parameterised by L (z) ~ L(0) (1+z)3.4. The environments of UBR selected AGN and radio galaxies have been measured at z~0.5 using the Panoramic Deep Field galaxy catalogue. By applying photometric red-shifts and colour selection criteria to the galaxy catalogue, it has been possible to increase the signal-to-noise of the angular correlation function and measure the cross-correlation with specific galaxy types. Most AGN host environments are comparable to the environments of galaxies with the same morphology. However, ~6% of UBR selected AGN are in significantly richer environments. No significant correlation between AGN luminosity and environment was detected in the Panoramic Deep Fields. The richness of AGN environments is not strongly correlated with redshift and the rapid evolution of the AGN luminosity function is not caused by evolution of AGN host environments.
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ItemA spectroscopic and chromatographic study of the photochemical properties of daylight fluorescent paint( 2009)Daylight fluorescent pigments fade rapidly, accompanied by a chronology of colour change. Fluorescence is a photo-physical phenomenon which involves emission of light from an excited state. Fluorescent dyes thus have a high susceptibility of being promoted to an excited state; a characteristic in the case of organic fluorophores which infers vulnerability toward photo-bleaching. Multiple organic fluorescent dyes are routinely incorporated into a given daylight fluorescent pigment, to either additively fluoresce or interact through energy transfer. The organic fluorescent dyes employed invariably differ in photo-stability, and upon loss of each species of fluorophore an abrupt colour change is observed. The collective result of this fading behaviour is that in a short period of time a daylight fluorescent paint layer will be of a different hue, devoid of luminosity. As consequence it is almost impossible to colour match a faded daylight fluorescent paint layer without the hues diverging asynchronously, or ascertain the original palette of a daylight fluorescent artwork after a protracted period of time. The predicament is exacerbated by the fact that there is no standard method in cultural material conservation, of documenting daylight fluorescent colour in a painting photographically or colorimetrically. The objective of this thesis is to investigate the photochemical behaviour of daylight fluorescent pigments, to ensure best practice in the preservation of artworks that contain daylight fluorescent paint. Fluorimetrie and chromatographic analysis of the DayGlo daylight fluorescent pigment range at the constituent dye level, prior to and during an accelerated light ageing program formed the basis of the experimental. Given the limited selection of fluorescent dyes suitable for daylight fluorescent pigment manufacture, it is anticipated that the results attained for the DayGlo range will be applicable to all daylight fluorescent media encountered in cultural material. Experimental data revealed the manner in which the fluorescent dyes behind each DayGlo daylight fluorescent pigment were formulated, and provided explanation for the 1colour changes observed upon fading. A prognosis of when and why a daylight fluorescent palette experiences hue shift and the implications this has for display is presented. Methodology for imaging daylight fluorescence, identification of the constituent fluorescent dyes in a daylight fluorescent pigment and colour matching a daylight fluorescent paint layer are presented and applied in-situ, to case studies possessing a daylight fluorescent palette.
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ItemAstigmatic phase retrieval of lightfields with helical wavefronts( 2012)The controlled use of coherent radiation has led to the development of a wide range of imaging methods in which aspects of the phase are enhanced through diffraction and propagation. A mathematical description of the propagation of light allows us to determine the properties of an optical wavefield in any plane. When a sample is illuminated with coherent planar illumination and its diffracted wavefield is recorded in the far-field of propagation, a direct inverse calculation of the phase can be quickly performed through computational means – the fast Fourier transform. Algorithmic processing is required, however, because only the intensity of the diffracted wavefield can be recorded. To determine structural information about the sample, some other information must be known about the experimental system. What is known, and how it is processed computationally, has led to the development and successful application of a broad spectrum of phase reconstruction iterative algorithms. Vortices in lightfields have a helical structure to their wavefront, at the core of which exists, necessarily, a screw-discontinuity to their phase. They have a characteristic intensity distribution comprising a radially symmetric bright ring around a dark core which, for either handedness of the rotation of the vortex, appears identical. Observation of a vortex is, therefore, ambiguous in its ability to determine its true direction of rotation. The ubiquitous presence of vortices in all lightfields hinder the success of phase reconstruction methods based on planar illumination and, if successful, render any reconstruction of the phase non-unique, due to the ambiguity associated to their helicity. The presence of a controlled spherical phase distortion can break the symmetry of the appearance of the vortices and, hence, remove the ambiguity from the system and drive algorithms to a solution. For the pathological case of an on-axis vortex, however, spherical distortion will not break the radial symmetry. The astigmatic phase retrieval method separates the spherical distortion into cylindrical distortion in two orthogonal directions. This form of phase distortion breaks the symmetry of a vortex allowing a unique determination of the phase. The incorporation of such use of cylindrical distortion into an iterative phase reconstruction algorithm forms the basis for the astigmatic phase retrieval (APR) method. Presented in this thesis is the creation and propagation of lightfields with helical wavefronts, produced through simulation and experiment. Observation of the effects of cylindrical distortion on vortices is explored in detail, particularly for split high-charge vortices where their positions can inform the type and strength of the applied phase distortion. Experimentally, onaxis vortices are created and distorted for the purposes of astigmatic phase retrieval in both visible light and X-ray wavefields. This thesis presents the first experimental demonstration of the astigmatic phase retrieval (APR) method, successfully applied optically with a simple test sample. The method is also applied to lightfields with helical wavefronts. The successful unambiguous reconstruction of on-axis chargeone and charge-two visible light vortices are presented, which is the first experimental demonstration on the unique phase reconstruction of an on-axis vortex from intensity measurements alone. Experiments are then performed to apply the method to vortices created in X-ray wavefields. The parameters of the experiment and the data have not, however, allowed for a successful reconstruction in this case. It is demonstrated through extensive simulation analysis that the APR method is a fast and robust imaging method. It is also shown that, through observation of the error metric, experimental parameters can be corrected or even determined, making the method successful even if there is no a priori knowledge of the experimental system. The application of the APR method as a general imaging technique for use in high-resolution X-ray diffraction experiments is, therefore, is a logical extension of the work of this thesis.
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ItemStudies for the adaptation of a field ionization ion source for a proton microprobe( 1989)A major factor limiting the resolution of the Scanning Proton Microprobe is the brightness of the primary beam supplied by the accelerator. The recent development of a field ionization proton source, which is up to five orders of magnitude brighter than the present source, holds the promise of substantially improved resolution in MP. The optics of the Pelletron accelerator were studied to determine the expected resolution improvement to the MP beam from the installation of the new source. The optics of the field ionization source region were studied using the charge simulation method. First order effective source size was calculated for field ionization tips, and calculations carried out to determine the contribution of aberrations to source size. Tip size and applied voltage to maximize source brightness were also investigated. The present electrostatic lens was investigated for use with the field ionization source, and found to be unsuitable unless very high voltages were to be applied. A range of alternative two and three element electrostatic lenses was investigated. Three element lenses were found to be more flexible, and generally had lower aberrations than two element lenses. Various designs of three element lenses were examined, and accelerating and decelerating modes discussed for all lenses. Accelerating lenses, although optically superior, were generally found to require unacceptably high applied voltages in order to achieve focusing. Decelerating lenses were investigated in further detail, and the geometry of promising lenses varied to attempt to reduce aberrations. Calculations suggested the best alternative to the present lens to be a miniaturized variation of the decelerating Riddle lens. A full scale version of this lens was studied on a specially constructed electron optical bench. The two grid method was used to measure cardinal points for the lens, as well as chromatic and spherical aberrations. The values of measured optical properties were found to correspond well with theoretical calculations for the same lens over the voltage range of most importance, suggesting that a reduced scale version of the same lens would be suitable for use with the field ionization source. The optics of the accelerating column were also investigated using the finite element method. Cardinal elements were extracted for a range of source lens operating voltages, permitting the calculation of accelerator object positions for a focus at the analysing magnet object slits. Chromatic and spherical aberrations of the accelerating column were also determined, and their effect on beam brightness for various source and lens configurations discussed. Finally all ion optical elements were combined and the final brightness, and expected MP beam resolution determined for a range of optical combinations Conclusions were drawn on the most appropriate optical configuration of the accelerator. Further work required for the installation of the source was also discussed.
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ItemApplication of a scanning proton microprobe as a diagnostic tool and the development of a high brightness ion source( 1989)This thesis concerns both the application and future development of a Scanning Proton Microprobe (SPMP). The work involved the use of a microprobe in a biological project which placed heavy demands on beam brightness, and also a program to investigate and address the demand for brighter microprobe beams. The thesis thus falls naturally into two distinct, though related, sections. The SPMP has been applied to the study of Menkes' disease, a copper-dependent genetic disorder. The disease is expressed in fibroblast cells, and the SPMP was used to map elemental distributions within both normal and Menkes' fibroblasts. An elevated level of intracellular copper was observed within Menkes' cells enabling individual cells to be identified as normal or Menkes' depending upon the copper content of the cell. Subcellular structure within fibroblasts was investigated by using the microprobe as a Scanning Transmission Ion Microscope (STIM). It was shown that this technique affords sufficient resolution to image the nuclear membrane and nucleoli. However, at this resolution, insufficient beam current was available to permit elemental distributions to be obtained. The elemental content of subcellular and subnuclear components is of fundamental importance to biochemical processes within the cell and to the expression of Menkes' disease. Hence an increase in the resolution of the SPMP is of major importance provided that the beam current can be maintained at levels acceptable for elemental analysis. Such a significant improvement in microprobe resolution can only be achieved with a brighter primary beam from the accelerator. This requires a brighter ion source. The performance of the existing RF ion source has been studied on a suitable test-bench, and its brightness measured. The possible use of alternative ion sources offering significant gains in. brightness was investigated, and an ion source using the process of field ionization was designed and built. Field ionization sources use a sharply pointed emitter as the site for ion production. This gives these sources an intrinsically high brightness, but in general they have not been designed so as to produce currents suitable for use in an electrostatic accelerator. The present field ionization source was optimized to produce a maximum current whilst being sufficiently rugged and compact to withstand use within the accelerator. The beam brightness achieved with this source offered a significant increase in source brightness with sufficient current to provide stable operation of the accelerator. The successful implementation of this source would produce a major improvement in the spatial resolution available for imaging and elemental analysis with the microprobe.