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    1,3-Dipolar Cycloaddition in the Preparation of New Fused Heterocyclic Compounds via Thermal Initiation

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    Author
    Porubsky, M; Tenora, L; Potacek, M
    Date
    2016-02-01
    Source Title
    Molecules
    Publisher
    MDPI
    Affiliation
    School of Chemistry
    Metadata
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    Document Type
    Journal Article
    Citations
    Porubsky, M., Tenora, L. & Potacek, M. (2016). 1,3-Dipolar Cycloaddition in the Preparation of New Fused Heterocyclic Compounds via Thermal Initiation. MOLECULES, 21 (2), https://doi.org/10.3390/molecules21020187.
    Access Status
    Open Access
    URI
    http://hdl.handle.net/11343/260370
    DOI
    10.3390/molecules21020187
    Abstract
    This paper describes the synthesis of precursors with a benzo[b]furan skeleton for the intramolecular 1,3-dipolar cycloaddition of azomethine ylides prepared from N-substituted 3-allyl-aminobenzo[b]furan-2-aldehydes and secondary amines derived from α-amino acid esters. Reactions were initiated by heating. The products consisted of four fused rings with three stereogenic centers. Their structure and stereochemistry were determined by NMR spectra and X-ray measurements.

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